Synthesis and Characterization of New Vic-dioximes and Their Nickel Complexes

Research Article

Tülay ÇAM* and Gaz

Abstract

In this study, four new vic-dioximes, anti-4-aminodiphenylaminoglyoxime (H2L1), anti-4-aminodiphenylaminophenylglyoxime (H2L2), anti-3-hydroxy-5-sulpho-2-naphthylaminoglyoxime (H3L3), and anti-3-hydroxy-5-sulpho-2-naphthylaminophenylglyoxime (H3L4), as well as their nickel complexes, were synthesized. The structures of these new compounds (both the ligands and complexes) were characterized by the following methods: IR, NMR, atomic absorption spectroscopy, elemental analysis, differential thermal analysis (DTA), and thermogravimetric analysis(TGA).

Relevant Publications in Der Chemica Sinica