Simultaneous Determination of Fluconazole and Tinidazole in Combined Dose Tablet using High Performance Thin Layer Chromatography

Research Article

Dhananjay B. Meshram, Priyanka

Abstract

This paper presents an HPTLC method, validated for simultaneous determination of fluconazole (FLZ) and tinidazole (TNZ) in a combined dose tablet. Chromatography was performed on silica gel 60F254 plates with 250 μm thickness, using Toluene: Ethyl acetate: Chloroform: Methanol (1.2:3:2:0.8 v/v) as a mobile phase. For the proposed method, linearity (FLZ-r2 > 0.996; TNZ-r2 > 0.997), sensitivity (FLZ-3.04 ng/spot; TNZ-11.12 ng/spot), recovery (FLZ- 98.66%-99.13%; TNZ- 99.26%-100.54%), and repeatability were found to be satisfactory. The HPTLC method offers a simple, sensitive, rapid and cost effective technique that can be applied successfully in routine quality control of formulations containing FLZ and TNZ.

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